將p-triallylcalix[4]arene（1）和對位含有不同取代的偶氮鹽類進行偶氮偶合反應，可形成相對應之對位丙烯基三取代及偶氮基單取之calix[4]arenas (2-6)。對這些calix[4]arene衍生物的合成及其核磁共振光譜之特性本文將有詳盡的探討。
Dizonium coupling between P-triallylcalix [4] arene (1) and p-substituted benzene-diazonium salts yielded the respective calix [4] arenas (2-6) with twodifferent substitutents on their para-position. The 1H-NMR spectral characteristic feature of these calix [4] arenes' derivatives are discussed.
